Simultaneous Determination of Inorganic Nitrogen Species in Seawater by Ion Chromatography —Addition Effect of EDTA to Seawater—

Determination of ammonium in seawater by column-switching ion chromatography.

A system which combines column switching and concentration was developed. A binary eluent mechanism was developed to study the effect of high sample concentration matrix on retention time shifts of the trace analyte. Separation conditions were chosen according to this mechanism to reduce the retention time shift of ammonium in the presence of high concentration sodium ion: high concentration su...

Determination of dissolved organic nitrogen in seawater using Kjeldahl digestion after inorganic nitrogen removal

RÉSUMÉ M. D. DOVAL *,Fernando FRAGA and Fiz F. PEREZ Instituto de Investigaciones Marinas de Vigo (CSIC), Eduardo Cabello, 6, E-36208 Vigo, Spain. * Corresponding author. E-mail:[email protected] Received 15/02/96, in revised form 04/12/96, accepted 16/01/97. An update of the Kjeldahl method is presented for the direct determination of dissolved organic nitrogen (DON) in seawater. Dissolved in...

Determination of iodide in seawater by capillary ion chromatography using hexadimethrine bromide modified C30 stationary phases.

A novel and simple capillary ion chromatographic method for the determination of iodide is reported. Separation was achieved on a laboratory-made packed capillary column (100 mm × 0.32 mm i.d.) packed with triacontyl-functionalized silica, followed by a modification with hexadimethrine bromide, where 1 mM sodium chloride-acetonitrile (95:5, v/v) was used as the eluent and UV-absorbing analyte ...

Fast direct determination of strontium in seawater using high-performance chelation ion chromatography

Ion chromatography for determination of nitrite and nitrate in seawater using monolithic ODS columns.

A fast and highly sensitive ion chromatographic method using monolithic ODS columns was developed for the determination of nitrite (NO2-) and nitrate (NO3-) in seawater. Two monolithic ODS columns (50 mm x 4.6 mm i.d. + 100 mm x 4.6 mm i.d.) connected in series were coated and equilibrated with 5 mM cetyltrimethylammonium chloride (CTAC) aqueous solution. The column efficiency with 0.5 M NaCl a...